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Erschienen in:
Computational Methods in Spectroscopy Kapitel lesen Erstes Kapitel lesen

2019 | OriginalPaper | Buchkapitel

4. Material Analysis Using Raman Spectroscopy

A Comparative Study of Graphite, Single- and Multi-walled Carbon Nanotubes

verfasst von : Animesh K. Ojha, H. Michael Heise

Erschienen in: Molecular Spectroscopy—Experiment and Theory

Verlag: Springer International Publishing

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Abstract

A comparative Raman spectroscopic study of single-walled carbon nanotubes (SWCNT), special multi-walled carbon nanotube (MWCNT) material, and graphite is presented. Their Raman spectra have been recorded using different excitation wavelengths, 532, 785, and 1064 nm, in the region of 1800–1200 cm−1. The G-bands of SWCNTs observed at all excitation wavelengths were fitted taking bands into account with Breit-Wigner-Fano (BWF) and Lorentzian line shape functions. The contribution of both BWF and Lorentzian line shapes to the asymmetric G-band shows a mixture of semiconducting as well as metallic CNTs in the SWCNTs. For graphite and MWCNTs, only Lorentzian line shape functions were used for band deconvolution. The variation in wavenumber position of component bands of G-band with laser lines may be due to the resonance Raman effect, where the energy of laser lines matches with the electronic transition energy of CNTs with different diameters and chirality. The apparent Young’s modulus of SWCNT and MWCNT materials was determined using the integrated band intensity ratio of G- and D-bands, ID/IG, and it was found that the SWCNTs have a larger value of the apparent Young’s modulus compared to that of the highly aligned MWCNT material.

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Metadaten
Titel
Material Analysis Using Raman Spectroscopy
verfasst von
Animesh K. Ojha
H. Michael Heise
Copyright-Jahr
2019
Buch
Molecular Spectroscopy—Experiment and Theory

Print ISBN: 978-3-030-01354-7

Electronic ISBN: 978-3-030-01355-4

Copyright-Jahr: 2019

DOI
https://doi.org/10.1007/978-3-030-01355-4_4

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