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Biomass Conversion and Biorefinery

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16.03.2022 | Original Article

Process optimization by response surface methodology-central composite design for the adsorption of lead by green synthesized TiO₂ using Phyllanthus acidus extract

verfasst von: Neethu Jayan, Laxmi Deepak Bhatlu Metta

Erschienen in: Biomass Conversion and Biorefinery | Ausgabe 1/2024

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Abstract

TiO₂ nanoparticles were synthesized using Phyllanthus acidus leaf extract. The presence of amines, aliphatic alcohol, phenolic acids and hydroxyl group in the Phyllanthus acidus leaf extract may be responsible for the reduction of TiO₂ nanoparticles from a precursor. Green synthesized TiO₂ nanoparticles were characterized with the help of UV–visible spectroscopy, XRD, FTIR, FESEM-EDX, TEM and BET analysis. The size of nanoparticles was determined to be 20–40 nm with a surface area of 108.31 m²/g, a pore size of 1.347 nm and a total pore volume of 0.1456 cc/g. The performance of heavy metal adsorption of TiO₂ nanoparticles was assessed. The process variables such as metal initial concentration, adsorbent dosage, pH and contact time for the adsorption of lead were optimized using response surface methodology (RSM) with central composite design (CCD). The lead removal efficiency of 98.6% was achieved using green synthesized TiO₂ nanoparticles under optimum conditions, an initial lead concentration of 89 mg/L, a dosage of adsorbent at 0.32 g, pH of 7.8 and a contact time of 89 min. The fitting of different isotherm models was carried out with the experimental and observed data, which confirmed that the Langmuir model best fit to describe the adsorption isotherm with an adsorption capacity of 2.633 mg/g. The first-order model is the optimum kinetic model, illustrating the rate of the equation of the adsorption of lead on TiO₂ nanoparticles.

Vorheriger Artikel A green way for pyruvic acid synthesis from biomass-derived L-malic acid on tetrahedral versus octahedral cobalt sites/hematite

Nächster Artikel Nanocoating of microbial fuel cell electrodes for enhancing bioelectricity generation from wastewater

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Titel: Process optimization by response surface methodology-central composite design for the adsorption of lead by green synthesized TiO2 using Phyllanthus acidus extract
verfasst von: Neethu Jayan
Laxmi Deepak Bhatlu Metta
Publikationsdatum: 16.03.2022
Verlag: Springer Berlin Heidelberg
Erschienen in: Biomass Conversion and Biorefinery / Ausgabe 1/2024
Print ISSN: 2190-6815
Elektronische ISSN: 2190-6823
DOI: https://doi.org/10.1007/s13399-022-02534-w

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