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Journal of Materials Engineering and Performance

Erschienen in:

01.01.2014

TiO₂-Bioactive Glass Nanostructure Composite Films Produced by a Sol-Gel Method: In Vitro Behavior and UV-Enhanced Bioactivity

verfasst von: Marzie Omid-Bakhtiari, Mojtaba Nasr-Esfahani, Abolghasem Nourmohamadi

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 1/2014

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Abstract

The aim of this study is to develop TiO₂, titania, -based composite films for 316 stainless steel substrate and to improve their apatite-forming activity. A series of sol-gel derived bioactive glass (49S) and bioactive glass (49S)-TiO₂ films were deposited on the 316L stainless steel substrates by the spin-coating method. Amorphous bioactive glass (49S) film and polycrystalline titania-bioactive glass composite films were obtained after annealing the deposited layers at 600 °C. The microstructure and in vitro bioactivity of the composite films as well as the effect of titania nanopowder content and ultra violet (UV) irradiation on the in vitro bioactivity were investigated by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). While bioactivity tests are often carried out within 28-day periods, SEM and EDS data show that, after soaking in SBF for just 7 days, the prepared composite surfaces are covered with an apatite layer. The grown apatite layer consists of spherulites formed by nanosized needle-like aggregates. Fourier transform infrared spectroscopy investigations confirm apatite formation and suggest that the formed apatite is carbonated.

Vorheriger Artikel On Microstructure and Microhardness of Isothermally Aged UNS S32760 and the Effect on Toughness and Corrosion Behavior

Nächster Artikel Synthesis and Properties of La2O3-Doped 8 mol% Yttria-Stabilized Cubic Zirconia

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Titel: TiO2-Bioactive Glass Nanostructure Composite Films Produced by a Sol-Gel Method: In Vitro Behavior and UV-Enhanced Bioactivity
verfasst von: Marzie Omid-Bakhtiari
Mojtaba Nasr-Esfahani
Abolghasem Nourmohamadi
Publikationsdatum: 01.01.2014
Verlag: Springer US
Erschienen in: Journal of Materials Engineering and Performance / Ausgabe 1/2014
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-013-0639-3

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