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01.04.2013 | Research Paper

A novel method for controlled synthesis of nanosized hematite (α-Fe₂O₃) thin film on liquid–vapor interface

verfasst von: Pawan Kumar, Raj Kumar Singh, Nitin Rawat, Partha Bir Barman, Subhash Chander Katyal, Hwanchol Jang, Heung-No Lee, Rajesh Kumar

Erschienen in: Journal of Nanoparticle Research | Ausgabe 4/2013

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Abstract

Hematite (α-Fe₂O₃) films with a high quality surface morphology have been formed at the liquid–vapor interface using a novel approach. The surface morphology/size of the nanoparticles constituting the film is tuned in a controlled manner. It is observed that the concentration of polyvinyl alcohol in the precursor Fe³⁺/Fe²⁺ solution, the concentration of ammonia (NH₃) vapor, and the annealing temperature are factors influencing the surface morphology/size of nanoparticles. The diameter of the α-Fe₂O₃ nanoparticles inside the film is controlled to be 2–15 nm by varying the synthesis conditions, and accordingly the films have roughness in the 1.34–6.8 nm range. The prepared α-Fe₂O₃ films are crystalline in nature and exhibit superparamagnetic behavior at room temperature.

Vorheriger Artikel Localized surface plasmon resonance (LSPR) study of DNA hybridization at single nanoparticle transducers

Nächster Artikel The role of polyaniline in the formation of iron-containing nanocomposites

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Titel: A novel method for controlled synthesis of nanosized hematite (α-Fe2O3) thin film on liquid–vapor interface
verfasst von: Pawan Kumar
Raj Kumar Singh
Nitin Rawat
Partha Bir Barman
Subhash Chander Katyal
Hwanchol Jang
Heung-No Lee
Rajesh Kumar
Publikationsdatum: 01.04.2013
Verlag: Springer Netherlands
Erschienen in: Journal of Nanoparticle Research / Ausgabe 4/2013
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI: https://doi.org/10.1007/s11051-013-1532-6

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