Skip to main content
Erschienen in: Journal of Materials Engineering and Performance 10/2021

17.06.2021

Boron-Doped Hydroxyapatite Coatings on NiTi Alloys Using the Electrophoretic Deposition Method: Enhanced Corrosion and Adhesion Performances

verfasst von: M. E. Aksoy, B. Aksakal, N. Aslan, B. Dikici

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 10/2021

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

Metallic implants are functionalized with coatings due to the need to protect against biological corrosion in the body. Hydroxyapatite (HAp) has desirable biocompatibility and structural properties, but poor mechanical properties limit its use as a standalone coating. In this study, boron-doped hydroxyapatite (B-HAp) biocomposites containing 5, 10, and 15% boron by weight were synthesized by the sol-gel method and applied as a coating to NiTi using electrophoretic deposition (EPD). The deposition was carried out for 60, 90, and 120 s, and sintering at 750 °C for 75 minutes under vacuum. The coated substrates were then characterized by XRD, SEM, and FT-IR, and their adhesion strengths and in-vitro corrosion behaviors in simulated body fluid were compared with uncoated samples. The results showed that the microporous powders formed well-bonded structures, which positively affect adhesion strength. The highest adhesion strength (30 MPa) and corrosion resistance were achieved with 15 wt.% B-HAP coating at 120 s deposition time and 76.5 μm coating thickness.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
3.
Zurück zum Zitat B. Dikici, Z. Esen, O. Duygulu, and S.G. (Koc), Corrosion of Metallic Biomaterials, Advances in Metallic Biomaterials: Tissues, Materials and Biological Reactions, M. Niinomi, T. Narushima, and M. Nakai, Eds., (Berlin, Heidelberg), Springer-Verlag Berlin Heidelberg, (2015), p 275–303, doi:https://doi.org/10.1007/978-3-662-46836-4 B. Dikici, Z. Esen, O. Duygulu, and S.G. (Koc), Corrosion of Metallic Biomaterials, Advances in Metallic Biomaterials: Tissues, Materials and Biological Reactions, M. Niinomi, T. Narushima, and M. Nakai, Eds., (Berlin, Heidelberg), Springer-Verlag Berlin Heidelberg, (2015), p 275–303, doi:https://​doi.​org/​10.​1007/​978-3-662-46836-4
5.
Zurück zum Zitat E. Ergun, C. Elmas, and N.E. Olcay, “Properties of Bioceramics Materials and Their Applications,” 10th Denizli Mater Symp and Exhibition, (Denizli, Turkey), Pamukkale Üniversitesi, (2004), p 25–41 E. Ergun, C. Elmas, and N.E. Olcay, “Properties of Bioceramics Materials and Their Applications,” 10th Denizli Mater Symp and Exhibition, (Denizli, Turkey), Pamukkale Üniversitesi, (2004), p 25–41
8.
Zurück zum Zitat D.M. Brunette, P. Tengvall, M. Textor, and P. Thomsen, “Titanium in Medicine: Material Science, Surface Science, Engineering, Biological Responses and Medical Applications,” (Berlin, Heidelberg), Springer Berlin Heidelberg, (2001), doi:https://doi.org/10.1007/978-3-642-56486-4 D.M. Brunette, P. Tengvall, M. Textor, and P. Thomsen, “Titanium in Medicine: Material Science, Surface Science, Engineering, Biological Responses and Medical Applications,” (Berlin, Heidelberg), Springer Berlin Heidelberg, (2001), doi:https://​doi.​org/​10.​1007/​978-3-642-56486-4
10.
Zurück zum Zitat B. Aksakal, M. Kom, H.B. Tosun and M. Demirel, Influence of Micro- and Nano-Hydroxyapatite Coatings on the Osteointegration of Metallic (Ti6Al4 V) and Bioabsorbable Interference Screws: An in Vivo Study, Eur. J. Orthop. Surg. Traumatol., 2014, 24(5), p 813–819. https://doi.org/10.1007/s00590-013-1236-8CrossRef B. Aksakal, M. Kom, H.B. Tosun and M. Demirel, Influence of Micro- and Nano-Hydroxyapatite Coatings on the Osteointegration of Metallic (Ti6Al4 V) and Bioabsorbable Interference Screws: An in Vivo Study, Eur. J. Orthop. Surg. Traumatol., 2014, 24(5), p 813–819. https://​doi.​org/​10.​1007/​s00590-013-1236-8CrossRef
16.
Zurück zum Zitat B. Dikici, M. Niinomi, M. Topuz, Y. Say, B. Aksakal, H. Yilmazer and M. Nakai, Synthesis and Characterization of Hydroxyapatite/TiO2 Coatings on the β-Type Titanium Alloys with Different Sintering Parameters Using Sol-Gel Method, Prot. Met. Phys. Chem. Surfaces, 2018, 54(3), p 457–462. https://doi.org/10.1134/S2070205118030255CrossRef B. Dikici, M. Niinomi, M. Topuz, Y. Say, B. Aksakal, H. Yilmazer and M. Nakai, Synthesis and Characterization of Hydroxyapatite/TiO2 Coatings on the β-Type Titanium Alloys with Different Sintering Parameters Using Sol-Gel Method, Prot. Met. Phys. Chem. Surfaces, 2018, 54(3), p 457–462. https://​doi.​org/​10.​1134/​S207020511803025​5CrossRef
17.
Zurück zum Zitat Y. Say, B. Aksakal and B. Dikici, Effect of Hydroxyapatite/SiO2 Hybride Coatings on Surface Morphology and Corrosion Resistance of REX-734 Alloy, Ceram Int., 2016, 42(8), p 10151–10158.CrossRef Y. Say, B. Aksakal and B. Dikici, Effect of Hydroxyapatite/SiO2 Hybride Coatings on Surface Morphology and Corrosion Resistance of REX-734 Alloy, Ceram Int., 2016, 42(8), p 10151–10158.CrossRef
18.
Zurück zum Zitat B. Aksakal, Y. Say, Ç. Buyukpinar and S. Bakirdere, Biodegradation of Hydroxyapatite Coated Rex-734 Alloy with Silver and Selenium/Chitosan Substitutions, Vitro Analysis. Ceram. Int., 2017, 43(15), p 12609–12615.CrossRef B. Aksakal, Y. Say, Ç. Buyukpinar and S. Bakirdere, Biodegradation of Hydroxyapatite Coated Rex-734 Alloy with Silver and Selenium/Chitosan Substitutions, Vitro Analysis. Ceram. Int., 2017, 43(15), p 12609–12615.CrossRef
21.
Zurück zum Zitat M. Mehrali, A.R. Akhiani, S. Talebian, M. Mehrali, S.T. Latibari, A. Dolatshahi-Pirouz, and H.S.C. Metselaar, Electrophoretic Deposition of Calcium Silicate-Reduced Graphene Oxide Composites on Titanium Substrate, J. Eur. Ceram. Soc., (2016). M. Mehrali, A.R. Akhiani, S. Talebian, M. Mehrali, S.T. Latibari, A. Dolatshahi-Pirouz, and H.S.C. Metselaar, Electrophoretic Deposition of Calcium Silicate-Reduced Graphene Oxide Composites on Titanium Substrate, J. Eur. Ceram. Soc., (2016).
31.
Zurück zum Zitat A. Wennerberg, C. Hallgren, C. Johansson, and S. Danelli, A Histomorphometric Evaluation of Screw-Shaped Implants Each Prepared with Two Surface Roughnesses, Clin. Oral Implants Res., (1998) A. Wennerberg, C. Hallgren, C. Johansson, and S. Danelli, A Histomorphometric Evaluation of Screw-Shaped Implants Each Prepared with Two Surface Roughnesses, Clin. Oral Implants Res., (1998)
32.
Zurück zum Zitat H. Farnoush, G. Aldıç and H. Çimenoğlu, Functionally Graded HA–TiO2 Nanostructured Composite Coating on Ti–6Al–4V Substrate via Electrophoretic Deposition, Surf. Coatings Technol., 2015, 265, p 7–15.CrossRef H. Farnoush, G. Aldıç and H. Çimenoğlu, Functionally Graded HA–TiO2 Nanostructured Composite Coating on Ti–6Al–4V Substrate via Electrophoretic Deposition, Surf. Coatings Technol., 2015, 265, p 7–15.CrossRef
35.
41.
Zurück zum Zitat D. Qiu, L. Yang, Y. Yin and A. Wang, Preparation and Characterization of Hydroxyapatite/Titania Composite Coating on NiTi Alloy by Electrochemical Deposition, Surf. Coatings Technol., 2011, 205(10), p 3280–3284.CrossRef D. Qiu, L. Yang, Y. Yin and A. Wang, Preparation and Characterization of Hydroxyapatite/Titania Composite Coating on NiTi Alloy by Electrochemical Deposition, Surf. Coatings Technol., 2011, 205(10), p 3280–3284.CrossRef
44.
Zurück zum Zitat C.T. Kwok, P.K. Wong, F.T. Cheng and H.C. Man, Characterization and Corrosion Behavior of Hydroxyapatite Coatings on Ti6Al4V Fabricated by Electrophoretic Deposition, Appl. Surf. Sci., 2009, 255(13–14), p 6736–6744.CrossRef C.T. Kwok, P.K. Wong, F.T. Cheng and H.C. Man, Characterization and Corrosion Behavior of Hydroxyapatite Coatings on Ti6Al4V Fabricated by Electrophoretic Deposition, Appl. Surf. Sci., 2009, 255(13–14), p 6736–6744.CrossRef
Metadaten
Titel
Boron-Doped Hydroxyapatite Coatings on NiTi Alloys Using the Electrophoretic Deposition Method: Enhanced Corrosion and Adhesion Performances
verfasst von
M. E. Aksoy
B. Aksakal
N. Aslan
B. Dikici
Publikationsdatum
17.06.2021
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 10/2021
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-021-05968-x

Weitere Artikel der Ausgabe 10/2021

Journal of Materials Engineering and Performance 10/2021 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.