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14.08.2020 | Original Article

Metal organic framework (ZIF-67)-derived Co nanoparticles/N-doped carbon nanotubes composites for electrochemical detecting of tert-butyl hydroquinone

verfasst von: Jing Tang, Sheng-Biao Zheng, Si-Xun Jiang, Jie Li, Teng Guo, Jia-Hao Guo

Erschienen in: Rare Metals | Ausgabe 2/2021

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Abstract

In this work, the framework of Co nanoparticles and nitrogen-doped carbon nanotubes (Co/NCNTs) derived from metal–organic frameworks (MOFs) through solid pyrolysis was successfully synthesized in the atmosphere of H₂ and Ar gases. The Co/NCNTs composites exhibited superior electrocatalytic performance for tert-butyl hydroquinone (TBHQ) oxidation due to the synergistic effect between chemical composition and the specific structure of Co nanoparticles and nitrogen-doped carbon nanotubes. It was found that the reaction underwent a quasi-reversible redox reaction with 37-fold higher anodic current for TBHQ at Co/NCNT-modified electrode when compared to bare glassy carbon electrode (GCE). In optimal condition, Co/NCNTs/GCE exhibited a linear range of 0.05–80.00 μmol·L⁻¹ for detecting TBHQ, and the limit of detection (LOD) was estimated to be as low as 10 nmol·L⁻¹ (signal/noise of S/N = 3). Moreover, the as-obtained modified electrode was successfully used to assay the content of TBHQ in edible oil samples.

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Vorheriger Artikel Facile fabrication of nanoscale hierarchical porous zeolitic imidazolate frameworks for enhanced toluene adsorption capacity

Nächster Artikel Two new pseudo-isomeric nickel (II) metal–organic frameworks with efficient electrocatalytic activity toward methanol oxidation

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Titel: Metal organic framework (ZIF-67)-derived Co nanoparticles/N-doped carbon nanotubes composites for electrochemical detecting of tert-butyl hydroquinone
verfasst von: Jing Tang
Sheng-Biao Zheng
Si-Xun Jiang
Jie Li
Teng Guo
Jia-Hao Guo
Publikationsdatum: 14.08.2020
Verlag: Nonferrous Metals Society of China
Erschienen in: Rare Metals / Ausgabe 2/2021
Print ISSN: 1001-0521
Elektronische ISSN: 1867-7185
DOI: https://doi.org/10.1007/s12598-020-01536-9

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