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Journal of Materials Engineering and Performance

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31.05.2022 | Technical Article

Structure and Electrochemical Behavior of AlN, AlTiN, and AlTiSiN Physical Vapor Deposition Coatings in 3% NaCl Solution

verfasst von: Anna Kameneva, Vladimir Kichigin, Natalia Bublik

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 12/2022

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Abstract

Thin coatings AlN, AlTiN, and AlTiSiN were deposited by pulsed magnetron sputtering. High-speed steel T1, structural carbon steel 1017, and hard alloy HG30 were used as substrates. The magnetron current, nitrogen content in the gas mixture, and bias voltage on the substrate were changed to obtain nanostructured and amorphous coating layers with different elemental compositions. The microstructure, defects, and elemental composition of the coatings were investigated on an Ultra 55 field emission electron microscope with an EDX microanalysis system. Voltammetry and impedance spectroscopy was performed on coated samples in 3% NaCl solution. The corrosion behavior of the coatings was characterized by the corrosion current density i_corr and the polarization resistance R_p (at the corrosion potential). The research shows that the investigated coatings (except for AlN) are electrochemically active, and corrosion processes occur not only on the substrate in the discontinuities of the coating but also on the coating surface. The corrosion current density for AlN and AlTiSiN coatings on a T1 substrate is about 0.1 μA cm⁻². The paper discusses factors influencing the corrosion behavior of the coatings under study.

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Vorheriger Artikel Investigation of the Crevice Corrosion Behavior of 316L Stainless Steel in Sulfate-Reducing Bacteria-Inoculated Artificial Seawater Using the Wire Beam Electrode

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Titel: Structure and Electrochemical Behavior of AlN, AlTiN, and AlTiSiN Physical Vapor Deposition Coatings in 3% NaCl Solution
verfasst von: Anna Kameneva
Vladimir Kichigin
Natalia Bublik
Publikationsdatum: 31.05.2022
Verlag: Springer US
Erschienen in: Journal of Materials Engineering and Performance / Ausgabe 12/2022
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-022-07030-w

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