nach oben

Journal of Materials Engineering and Performance

Erschienen in:

06.01.2022 | Technical Article

Assessment of 3D Printings Produced in Fused Deposition Modeling Printer Using Polylactic Acid/TiO₂/Hydroxyapatite Composite Filaments

verfasst von: Mikail Olam, Nihat Tosun

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 6/2022

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config

KI-gestützte Suche

Aus

Abstract

Polymer composite filaments, which consist of polylactic acid (PLA), titanium dioxide (TiO₂), synthetic hydroxyapatite (HA) and natural hydroxyapatite (NHA), have been produced via an extruder for using in biomedical applications. Then, 3D printings were produced in a fused deposition modeling (FDM) printer by using these composite filaments. A number of experiments and measurements were made on 3D printed PLA/HA/NHA/TiO₂ composite samples. According to the stress–strain analysis of 3D printing samples of PLA/HA/NHA/TiO₂ composites, the highest ultimate tensile strength, elastic modulus and elongation at break were 62, 1887 MPa, and 1.76 mm, respectively. According to SEM analysis, HA in PLA contributed to the spread of raster lines, and TiO₂ contributed to the smoothness of the raster lines. According to the dimensional accuracy analysis of the composites, the least deviation value was obtained in the samples 3D printed with 95%PLA/2.5%HA/2.5%TiO₂ filament at 205 °C extruder temperature. The lowest average roughness value of 95%PLA/4%HA/1%TiO₂ composite was 3 µm in the Z-axis plane. According to the data obtained, the extruder temperature is 220 °C, the printing speed is 2880 mm/min, the mixing ratio 95% PLA/4% HA/1% TiO₂ can be selected for optimal performance characteristics.

Vorheriger Artikel New Insight on the Effect of Yttria-Based Secondary Phases on Sintering and Electrical Behavior of Aluminum Nitride Ceramics

Nächster Artikel Titanium Electrical Resistivity in Hydrogen and Deuterium

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

über 102.000 Bücher
über 537 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Finance + Banking
Management + Führung
Marketing + Vertrieb
Maschinenbau + Werkstoffe
Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

über 67.000 Bücher
über 390 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Maschinenbau + Werkstoffe

Jetzt Wissensvorsprung sichern!

Jetzt informieren

K. Gnanasekaran, T. Heijmans, S. van Bennekom, H. Woldhuis, S. Wijnia, G. de With and H. Friedrich, 3D Printing of CNT- and Graphene-Based Conductive Polymer Nanocomposites by Fused Deposition Modeling, Appl. Mater. Today, 2017, 9, p 21–28.CrossRef

P.H.M. Cardoso, M.F.L. Oliveira, M.G. Oliveira, R.M. da Silva Moreira and Thiré, 3D Printed Parts of Polylactic Acid Reinforced with Carbon Black and Alumina Nanofillers for Tribological Applications, Macromol. Symp., 2020, 394(1), p 2000155. https://doi.org/10.1002/masy.202000155CrossRef

P. Parandoush and D. Lin, A Review on Additive Manufacturing of Polymer-Fiber Composites, Composite Structures, 2017, 182, p 36–53.CrossRef

Y. Jin, Y. He, J. Fu, W. Gan and Z. Lin, Optimization of Tool-Path Generation for Material Extrusion-Based Additive Manufacturing Technology, Addit. Manuf., 2014, 1–4, p 32–47. https://doi.org/10.1016/j.addma.2014.08.004CrossRef

O.A. Mohamed, S.H. Masood, J.L. Bhowmik and A.E. Somers, Investigation on the Tribological Behavior and Wear Mechanism of Parts Processed by Fused Deposition Additive Manufacturing Process, J. Manuf. Process., 2017, 29, p 149–159.CrossRef

N. Hossain, M.A. Chowdhury, M.B.A. Shuvho, M.A. Kashem and M. Kchaou, (2021) 3D-Printed Objects for Multipurpose Applications, J. Mater. Eng. Perform., 2021, 30(7), p 4756–4767. https://doi.org/10.1007/S11665-021-05664-WCrossRef

J. Torres, M. Cole, A. Owji, Z. DeMastry and A.P. Gordon, An Approach for Mechanical Property Optimization of Fused Deposition Modeling with Polylactic Acid via Design of Experiments, Rapid Prototyp. J., 2016, 22(2), p 387–404.CrossRef

A.K. Sood, R.K. Ohdar and S.S. Mahapatra, Experimental Investigation and Empirical Modelling of FDM Process for Compressive Strength Improvement, J. Adv. Res., 2012, 3(1), p 81–90.CrossRef

A.K. Sood, R.K. Ohdar and S.S. Mahapatra, Parametric Appraisal of Mechanical Property of Fused Deposition Modelling Processed Parts, Mater. Des., 2010, 31(1), p 287–295.CrossRef

10.

G. Strnad, R. Cazacu, P. Chetan, A.S. Gaz Florea, and F. Peti, “Effect of Phosphate/Fluoride Electrolytes on Mass and Dimensional Stability of Anodization Bath Manufactured by FDM,” MATEC Web of Conferences, EDP Sciences, 2017.

11.

A.P. Valerga, M. Batista, R. Puyana, A. Sambruno, C. Wendt and M. Marcos, Preliminary Study of PLA Wire Colour Effects on Geometric Characteristics of Parts Manufactured by FDM, Proc. Manuf., 2017, 13, p 924–931.

12.

S. Wang, D.R. D’hooge, L. Daelemans, H. Xia, K. De Clerck and L. Cardon, The Transferability and Design of Commercial Printer Settings in Pla/Pbat Fused Filament Fabrication, Polymers (Basel)., 2020, 12(11), p 1–20.

13.

T.C. Yang and C.H. Yeh, Morphology and Mechanical Properties of 3D Printed Wood Fiber/Polylactic Acid Composite Parts Using Fused Deposition Modeling (FDM): The Effects of Printing Speed, Polymers (Basel)., 2020, 12(6), p 1334.CrossRef

14.

A. Selvam, S. Mayilswamy, R. Whenish, R. Velu and B. Subramanian, Preparation and Evaluation of the Tensile Characteristics of Carbon Fiber Rod Reinforced 3D Printed Thermoplastic Composites, J. Compos. Sci., 2020, 5(1), p 8.CrossRef

15.

B. Coppola, N. Cappetti, L. Di Maio, P. Scarfato and L. Incarnato, Materials 3D Printing of PLA/Clay Nanocomposites: Influence of Printing Temperature on Printed Samples Properties, Materials, 2018 https://doi.org/10.3390/ma11101947CrossRef

16.

C. Abeykoon, P. Sri-Amphorn and A. Fernando, Optimization of Fused Deposition Modeling Parameters for Improved PLA and ABS 3D Printed Structures, Int. J. Light. Mater. Manuf., 2020, 3(3), p 284–297. https://doi.org/10.1016/j.ijlmm.2020.03.003CrossRef

17.

Y. Tao and L. Pan, Improving Tensile Properties of Polylactic Acid Parts by Adjusting Printing Parameters of Open Source 3D Printers, MEDŽIAGOTYRA, 2020 https://doi.org/10.5755/j01.ms.26.1.20952CrossRef

18.

T. Vukasovic, J.F. Vivanco, D. Celentano and C. García-Herrera, Characterization of the Mechanical Response of Thermoplastic Parts Fabricated with 3D Printing, Int. J. Adv. Manuf. Technol, 2019, 104(9–12), p 4207–4218.CrossRef

19.

T. Yao, Z. Deng, K. Zhang and S. Li, A Method to Predict the Ultimate Tensile Strength of 3D Printing Polylactic Acid (PLA) Materials with Different Printing Orientations, Compos. Part B Eng., 2019, 163, p 393–402.CrossRef

20.

B. Akhoundi and A.H. Behravesh, Effect of Filling Pattern on the Tensile and Flexural Mechanical Properties of FDM 3D Printed Products, Exp. Mech., 2019, 59(6), p 883–897. https://doi.org/10.1007/s11340-018-00467-yCrossRef

21.

G. Wang, D. Zhang, B. Li, G. Wan, G. Zhao and A. Zhang, Strong and Thermal-Resistance Glass Fiber-Reinforced Polylactic Acid (PLA) Composites Enabled by Heat Treatment, Int. J. Biol. Macromol., 2019, 129, p 448–459. https://doi.org/10.1016/j.ijbiomac.2019.02.020CrossRef

22.

S. Lin Yang, Z.H. Wu, W. Yang and M.B. Yang, Thermal and Mechanical Properties of Chemical Crosslinked Polylactide (PLA), Polym. Test., 2008, 27(8), p 957–963.CrossRef

23.

P. Törmälä, S. Vainionpää, J. Kilpikari and P. Rokkanen, The Effects of Fibre Reinforcement and Gold Plating on the Flexural and Tensile Strength of PGA/PLA Copolymer Materials in Vitro, Biomaterials, 1987, 8(1), p 42–45.CrossRef

24.

S. Ochi, Mechanical Properties of Kenaf Fibers and Kenaf/PLA Composites, Mech. Mater., 2008, 40(4–5), p 446–452. https://doi.org/10.1016/j.mechmat.2007.10.006CrossRef

25.

B. Bax and J. Müssig, Impact and Tensile Properties of PLA/Cordenka and PLA/Flax Composites, Composites Science and Technology, 2008, 68, p 1601–1607.CrossRef

26.

R. Auras, B. Harte and S. Selke, An Overview of Polylactides as Packaging Materials, Macromolecular Bioscience, 2004 https://doi.org/10.1002/mabi.200400043CrossRef

27.

J. Torres, J. Cotelo, J. Karl and A.P. Gordon, Mechanical Property Optimization of FDM PLA in Shear with Multiple Objectives, JOM, 2015, 67(5), p 1183–1193. https://doi.org/10.1007/s11837-015-1367-yCrossRef

28.

R. Aziz, M.I. Ul Haq and A. Raina, Effect of Surface Texturing on Friction Behaviour of 3D Printed Polylactic Acid (PLA), Polym. Test, 2020 https://doi.org/10.1016/j.polymertesting.2020.106434CrossRef

29.

M.H. Helal, H.D. Hendawy, R.A. Gaber, N.R. Helal and M.N. Aboushelib, Osteogenesis Ability of CAD-CAM Biodegradable Polylactic Acid Scaffolds for Reconstruction of Jaw Defects, J. Prosthet. Dent., 2019, 121(1), p 118–123.CrossRef

30.

E.V. Melnik, S.N. Shkarina, S.I. Ivlev, V. Weinhardt, T. Baumbach, M.V. Chaikina, M.A. Surmeneva and R.A. Surmenev, In Vitro Degradation Behaviour of Hybrid Electrospun Scaffolds of Polycaprolactone and Strontium-Containing Hydroxyapatite Microparticles, Polym. Degrad. Stab., 2019, 167, p 21–32.CrossRef

31.

M. Sadat-Shojai, M.T. Khorasani, E. Dinpanah-Khoshdargi and A. Jamshidi, Synthesis Methods for Nanosized Hydroxyapatite with Diverse Structures, Acta Biomaterialia, 2013, 9, p 7591–7621.CrossRef

32.

G. Montalbano, G. Molino, S. Fiorilli and C. Vitale-Brovarone, Synthesis and Incorporation of Rod-like Nano-Hydroxyapatite into Type I Collagen Matrix: A Hybrid Formulation for 3D Printing of Bone Scaffolds, J. Eur. Ceram. Soc., 2020, 40(11), p 3689–3697.CrossRef

33.

T.T. Hoai, N.K. Nga, L.T. Giang, T.Q. Huy, P.N.M. Tuan and B.T.T. Binh, Hydrothermal Synthesis of Hydroxyapatite Nanorods for Rapid Formation of Bone-Like Mineralization, J. Electron. Mater., 2017, 46(8), p 5064–5072.CrossRef

34.

J. Li, X.L. Lu and Y.F. Zheng, Effect of Surface Modified Hydroxyapatite on the Tensile Property Improvement of HA/PLA Composite, Appl. Surf. Sci., 2008, 255(2), p 494–497.CrossRef

35.

M. Luna, J. Delgado, M. Gil and M. Mosquera, TiO2-SiO2 Coatings with a Low Content of AuNPs for Producing Self-Cleaning Building Materials, Nanomaterials, 2018, 8(3), p 177. https://doi.org/10.3390/nano8030177CrossRef

36.

D. Colangiuli, M. Lettieri, M. Masieri and A. Calia, Field Study in an Urban Environment of Simultaneous Self-Cleaning and Hydrophobic Nanosized TiO2-Based Coatings on Stone for the Protection of Building Surface, Sci. Total Environ., 2019, 650, p 2919–2930.CrossRef

37.

M. Murugan, R. Subasri, T.N. Rao, A.S. Gandhi and B.S. Murty, Synthesis, Characterization and Demonstration of Self-Cleaning TiO 2 Coatings on Glass and Glazed Ceramic Tiles, Prog. Org. Coatings, 2013, 76(12), p 1756–1760.CrossRef

38.

C. Sciancalepore, T. Manfredini and F. Bondioli, Antibacterial and Self-Cleaning Coatings for Silicate Ceramics: A Review, Adv. Sci. Technol., 2014, 92, p 90–99. https://doi.org/10.4028/www.scientific.net/ast.92.90CrossRef

39.

P. Evans and D.W. Sheel, Photoactive and Antibacterial TiO2 Thin Films on Stainless Steel, Surf. Coatings Technol., 2007, 201, p 9319–9324.CrossRef

40.

N. Sykaras, A.M. Iacopino, V.A. Marker, R.G. Triplett, and R.D. Woody, Implant Materials, Designs, and Surface Topographies: Their Effect on Osseointegration. A Literature Review., Int. J. Oral Maxillofac. Implants, n.d., 15(5), p 675–90, http://www.ncbi.nlm.nih.gov/pubmed/11055135. Accessed 9 November 2020.

41.

L.M. Bjursten, L. Rasmusson, S. Oh, G.C. Smith, K.S. Brammer and S. Jin, Titanium Dioxide Nanotubes Enhance Bone Bonding in Vivo, J. Biomed. Mater. Res. - Part A, 2010, 92(3), p 1218–1224.

42.

T.-C. Yang, Effect of Extrusion Temperature on the Physico-Mechanical Properties of Unidirectional Wood Fiber-Reinforced Polylactic Acid Composite (WFRPC) Components Using Fused Deposition Modeling, Polymers, 2018, 10(9), p 976. https://doi.org/10.3390/POLYM10090976CrossRef

43.

S. Cheng, K. Tak Lau, T. Liu, Y. Zhao, P.M. Lam and Y. Yin, Mechanical and Thermal Properties of Chicken Feather Fiber/PLA Green Composites, Compos. Part B Eng., 2009, 40(7), p 650–654.CrossRef

44.

R. Singh, P. Bedi, F. Fraternali and I.P.S. Ahuja, Effect of Single Particle Size, Double Particle Size and Triple Particle Size Al2O3 in Nylon-6 Matrix on Mechanical Properties of Feed Stock Filament for FDM, Compos. Part B Eng., 2016, 106, p 20–27. https://doi.org/10.1016/j.compositesb.2016.08.039CrossRef

45.

N. Naveed, Investigate the Effects of Process Parameters on Material Properties and Microstructural Changes of 3D-Printed Specimens Using Fused Deposition Modelling (FDM), Mater. Technol., 2020, 36, p 317–330.CrossRef

46.

S.E. Nájera, M. Michel and N.-S. Kim, 3D Printed PLA/PCL/TiO2 Composite for Bone Replacement and Grafting, MRS Adv., 2018, 3(40), p 2373–2378. https://doi.org/10.1557/adv.2018.375CrossRef

47.

D. Hodzic and A. Pandzic, “Influence of Carbon Fibers on Mechanical Properties of Materials in Fdm Technology,” Annals of DAAAM and Proceedings of the International DAAAM Symposium, Danube Adria Association for Automation and Manufacturing, DAAAM, 2019, p 334–342.

48.

E. García Plaza, P. Núñez López, M. Caminero Torija and J. Chacón Muñoz, Analysis of PLA Geometric Properties Processed by FFF Additive Manufacturing: Effects of Process Parameters and Plate-Extruder Precision Motion, Polymers Basel., 2019, 11(10), p 1581. https://doi.org/10.3390/polym11101581CrossRef

49.

K. Tiwari and S. Kumar, Analysis of the Factors Affecting the Dimensional Accuracy of 3D Printed Products, Mater. Today: Proc., 2018, 5, p 18674–18680.

50.

V. Taşdemir, Investigation of Dimensional Integrity and Surface Quality of Different Thin-Walled Geometric Parts Produced via Fused Deposition Modeling 3D Printing, J. Mater. Eng. Perform., 2021, 30(5), p 3381–3387. https://doi.org/10.1007/S11665-021-05809-XCrossRef

Titel: Assessment of 3D Printings Produced in Fused Deposition Modeling Printer Using Polylactic Acid/TiO2/Hydroxyapatite Composite Filaments
verfasst von: Mikail Olam
Nihat Tosun
Publikationsdatum: 06.01.2022
Verlag: Springer US
Erschienen in: Journal of Materials Engineering and Performance / Ausgabe 6/2022
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-021-06539-w

Premium Partner

Marktübersichten

Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.

Zur Marktübersicht

Springer Professional

Abstract

Bitte loggen Sie sich ein, um Zugang zu Ihrer Lizenz zu erhalten.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Springer Professional "Technik"

Weitere Artikel der Ausgabe 6/2022

Probing High-Temperature Electrochemical Corrosion of 316 Stainless Steel in Molten Nitrate Salt for Concentrated Solar Power Plants

Experimental Investigation and Prediction of Mild Steel Turning Performances Using Hybrid Deep Convolutional Neural Network-Based Manta-Ray Foraging Optimizer

CO2-O2-SRB-Cl− Multifactor Synergistic Corrosion in Shale Gas Pipelines at a Low Liquid Flow Rate

Research on Adding Nano-SiC Reinforced Wire Arc Additive Manufacturing Stainless Steel

Microstructure, Mechanical Properties, and Cytotoxicity of β-Type Ti-Nb-Cr Alloys Designed by Electron Parameter

Comparison of 3D Printed Underwater Propeller Using Polymers and Conventionally Developed AA6061

Premium Partner

Marktübersichten