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Cellulose

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21.01.2020 | Original Research

Cationic modification of nanocrystalline cellulose from sago fronds

verfasst von: I. Wayan Arnata, Suprihatin Suprihatin, Farah Fahma, Nur Richana, Titi Candra Sunarti

Erschienen in: Cellulose | Ausgabe 6/2020

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Abstract

Sago fronds are agricultural waste, whose availability is enormous in Indonesia, yet not optimally utilized. This research was conducted to isolate nanocrystalline cellulose from sago frond material, using sulfuric acid, with variations in hydrolysis times and cationic modifications of the nanocrystalline cellulose surface. The profiles of Fourier transform infrared spectroscopy, a scanning electron microscopy, and X-ray diffraction indicated a decrease in lignin content, hemicellulose, and fiber dimensions, during the delignification, bleaching, and hydrolysis, followed by an increase in the cellulose content and in degrees of crystallinity. The variations in hydrolysis times affected the cellulosic nanocrystalline characteristics. Longer hydrolysis times caused a decrease in the yield, thermal stability, dimensions of nanocrystalline cellulose, and an increase in the degree of crystallinity and surface charge. The modification of nanocrystalline cellulose, using cetyltrimethylammonium bromide and 3-chloro-2-hydroxypropyltrimethylammonium chloride, led to the surface of nanocrystalline cellulose becoming positively charged followed by a decrease in the degree of crystallinity and thermal stability. The resulting nanocellulose had moderate stability and the potential to be applied in wider-scaled material processing.

Vorheriger Artikel Monitoring of cellulose oxidation level by electrokinetic phenomena and numeric prediction model

Nächster Artikel Factors affecting the hydrolytic action of xylanase during pennisetum saccharification: role of lignin

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Titel: Cationic modification of nanocrystalline cellulose from sago fronds
verfasst von: I. Wayan Arnata
Suprihatin Suprihatin
Farah Fahma
Nur Richana
Titi Candra Sunarti
Publikationsdatum: 21.01.2020
Verlag: Springer Netherlands
Erschienen in: Cellulose / Ausgabe 6/2020
Print ISSN: 0969-0239
Elektronische ISSN: 1572-882X
DOI: https://doi.org/10.1007/s10570-019-02955-3

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