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Erschienen in: Journal of Nanoparticle Research 10/2011

01.10.2011 | Research Paper

Photochemical preparation of ZnO nanoparticles

verfasst von: Tomáš Gbur, Václav Čuba, Viliam Múčka, Martin Nikl, Karel Knížek, Milan Pospíšil, Ivo Jakubec

Erschienen in: Journal of Nanoparticle Research | Ausgabe 10/2011

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Abstract

Preparation of zinc oxide nanoparticles from aqueous solutions containing zinc nitrate or formate using UV irradiation was investigated. Analysis of solid phase formed during irradiation confirmed the presence of zinc oxide or zinc peroxide nanoparticles ranging in size from 1 to 70 nm, depending on initial precursors. Annealing at temperatures 650–1000 °C results in forming of rice-like zinc oxide particles, up to hundreds of nm in size. Photochemical method yields material with high chemical purity and uniform particle size distribution. In addition, photo-induced doping of zinc oxide with lanthanum was studied. Presence of lanthanum in zinc oxide crystal lattice and post-preparation treatment in reduction atmosphere significantly increase the UV excitonic luminescence at 395 nm in radioluminescence spectra.

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Metadaten
Titel
Photochemical preparation of ZnO nanoparticles
verfasst von
Tomáš Gbur
Václav Čuba
Viliam Múčka
Martin Nikl
Karel Knížek
Milan Pospíšil
Ivo Jakubec
Publikationsdatum
01.10.2011
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 10/2011
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-011-0407-y

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