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Metallurgical and Materials Transactions B
Erschienen in: Metallurgical and Materials Transactions B 6/2018

24.08.2018

Microsegregation Measurement: Methods and Applications

verfasst von: Richard Smith

Erschienen in: Metallurgical and Materials Transactions B | Ausgabe 6/2018

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Abstract

Microsegregation is chemical variation at the microstructural level in a solidified ingot, which can cause undesirable effects on material properties. Its formation is driven by different levels of solute elemental solubility between solid and liquid phases, resulting in solute buildup or depletion in the liquid phase during solidification. Characterization of microsegregation can be essential for understanding its formation and removing it through heat treatment. Measurement is frequently carried out via scanning electron microscope (SEM), though metallographic analysis, mechanical testing and optical radiography have been used. SEM analysis can consist of point measurements on single dendrites, line scans across or along dendrites, elemental maps, and extended line-based or grid-based analyses extending over many dendrites, which can generate large amounts of data. Line-based or grid-based data can be analyzed using scatterplots of element concentrations to visualize segregation behavior and sorting/ranking of data by a single element or a combination of elements, to give compositional profiles as a function of extent of solidification. For both qualitative and quantitative analyses, effects of phase transformations and secondary phases need to be considered as well as sorting of measurement errors when generating compositional profiles. Applications of analysis include determination of partition ratios, examination of solute–element interactions, determination of effects of cooling rate and back diffusion, applications to freckling studies, validations of modeling, and development of heat-treatment profiles.
Vorheriger Artikel Thermomechanical Processing of Metal Feedstock for Semisolid Forming: A Review
Nächster Artikel Effects of Inclusion Precipitation, Partition Coefficient, and Phase Transition on Microsegregation for High-Sulfur Steel Solidification

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Metadaten
Titel
Microsegregation Measurement: Methods and Applications
verfasst von
Richard Smith
Publikationsdatum
24.08.2018
Verlag
Springer US
Erschienen in
Metallurgical and Materials Transactions B / Ausgabe 6/2018
Print ISSN: 1073-5615
Elektronische ISSN: 1543-1916
DOI
https://doi.org/10.1007/s11663-018-1395-4

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