Skip to main content
Erschienen in: Journal of Materials Engineering and Performance 12/2022

18.05.2022 | Technical Article

Fracture Behavior of GTD-111 Superalloy during In Situ Tensile Scanning Electron Microscopy

verfasst von: Yinwei Wang, Pengchao Zhang, Morteza Taheri, Behzad Babaei

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 12/2022

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

The deformation phenomenon and the fracture mechanism of the GTD-111 superalloy processed by selective laser melting were evaluated by in situ tensile scanning electron microscopy at 730 °C. Grain rotation and grain boundary slip were the most important mechanisms that occurred before fracture. As the grain boundary slip increased, holes and micro-cracks nucleated in the grain boundary. These micro-cracks extend into the grain, causing inter-granular fracture. At strains above 9%, micro-cracks occurred in the TiC carbides scattered within the grains, resulting in a change in fracture direction from grain boundary to inter-granular. The accumulation of dislocations behind the γ′ phase and the grain boundaries provided the driving force needed to start and propagate the crack.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat M. Taheri, A. Halvaee, and S.F. Kashani-Bozorg, Effect of Pre- and Post-Weld Heat Treatment on Microstructure and Mechanical Properties of GTD-111 Superalloy Welds, Met. Mater. Int., 2021, 27(5), p 1173–1192. CrossRef M. Taheri, A. Halvaee, and S.F. Kashani-Bozorg, Effect of Pre- and Post-Weld Heat Treatment on Microstructure and Mechanical Properties of GTD-111 Superalloy Welds, Met. Mater. Int., 2021, 27(5), p 1173–1192. CrossRef
2.
Zurück zum Zitat Q. Shen, X. Kong, X. Chen, X. Yao, V.B. Deev, and E.S. Prusov, Powder Plasma Arc Additive Manufactured CoCrFeNi (SiC) x High-Entropy Alloys: Microstructure and Mechanical Properties, Mater. Lett., 2021, 282, p 128736. CrossRef Q. Shen, X. Kong, X. Chen, X. Yao, V.B. Deev, and E.S. Prusov, Powder Plasma Arc Additive Manufactured CoCrFeNi (SiC) x High-Entropy Alloys: Microstructure and Mechanical Properties, Mater. Lett., 2021, 282, p 128736. CrossRef
3.
Zurück zum Zitat M. Taheri, A. Rasoulpouraghdam, A. Lohrasbi-Nejad, S.F. Kashani-Bozorg, and R.P. Liavoli, Influence of Heat Treatment on Creep Behavior of IN625 Coating on a Ni3Al-Base Superalloy, Mater. Res. Express, 2021, 8(5), p 056503. CrossRef M. Taheri, A. Rasoulpouraghdam, A. Lohrasbi-Nejad, S.F. Kashani-Bozorg, and R.P. Liavoli, Influence of Heat Treatment on Creep Behavior of IN625 Coating on a Ni3Al-Base Superalloy, Mater. Res. Express, 2021, 8(5), p 056503. CrossRef
4.
Zurück zum Zitat L. Qin, J. Wang, Q. Wu, X. Guo, and J. Tao, In-Situ Observation of Crack Initiation and Propagation in Ti/Al Composite Laminates During Tensile Test, J. Alloys Compd., 2017, 712, p 69–75. CrossRef L. Qin, J. Wang, Q. Wu, X. Guo, and J. Tao, In-Situ Observation of Crack Initiation and Propagation in Ti/Al Composite Laminates During Tensile Test, J. Alloys Compd., 2017, 712, p 69–75. CrossRef
5.
Zurück zum Zitat S. Wang, Y. Zhang, C. Schuman, J.S. Lecomte, X. Zhao, L. Zuo, and C. Esling, Study of Twinning/Detwinning Behaviors of Ti by Interrupted In Situ Tensile Tests, Acta Mater., 2015, 82, p 424–436. CrossRef S. Wang, Y. Zhang, C. Schuman, J.S. Lecomte, X. Zhao, L. Zuo, and C. Esling, Study of Twinning/Detwinning Behaviors of Ti by Interrupted In Situ Tensile Tests, Acta Mater., 2015, 82, p 424–436. CrossRef
6.
Zurück zum Zitat Y. Cao, N. Farouk, M. Taheri, A.V. Yumashev, S.F.K. Bozorg, and O.O. Ojo, Evolution of Solidification and Microstructure in Laser-Clad IN625 Superalloy Powder on GTD-111 Superalloy, Surf. Coat. Technol., 2021, 412, p 127010. CrossRef Y. Cao, N. Farouk, M. Taheri, A.V. Yumashev, S.F.K. Bozorg, and O.O. Ojo, Evolution of Solidification and Microstructure in Laser-Clad IN625 Superalloy Powder on GTD-111 Superalloy, Surf. Coat. Technol., 2021, 412, p 127010. CrossRef
7.
Zurück zum Zitat R. Bertrand, O. Caty, V. Mazars, S. Denneulin, P. Weisbecker, J. Pailhes, and F. Rebillat, In-Situ Tensile Tests Under SEM and X-Ray Computed Micro-Tomography Aimed at Studying a Self-Healing Matrix Composite Submitted to Different Thermomechanical Cycles, J. Eur. Ceram. Soc., 2017, 37(10), p 3471–3474. CrossRef R. Bertrand, O. Caty, V. Mazars, S. Denneulin, P. Weisbecker, J. Pailhes, and F. Rebillat, In-Situ Tensile Tests Under SEM and X-Ray Computed Micro-Tomography Aimed at Studying a Self-Healing Matrix Composite Submitted to Different Thermomechanical Cycles, J. Eur. Ceram. Soc., 2017, 37(10), p 3471–3474. CrossRef
8.
Zurück zum Zitat A. Lall, P. Bowen, and A. Rabiei, A Numerical and Experimental Approach to Compare the Effect of Sample Thickness in Small In-Situ SEM and Large Ex-Situ Tensile Testing in Alloy 709, Mater. Charact., 2022, 184, p 111614. CrossRef A. Lall, P. Bowen, and A. Rabiei, A Numerical and Experimental Approach to Compare the Effect of Sample Thickness in Small In-Situ SEM and Large Ex-Situ Tensile Testing in Alloy 709, Mater. Charact., 2022, 184, p 111614. CrossRef
9.
Zurück zum Zitat X. Liu, Y. Liu, B. Jin, Y. Lu, and J. Lu, Microstructure Evolution and Mechanical Properties of a SMATed Mg Alloy Under In Situ SEM Tensile Testing, J. Mater. Sci. Technol., 2017, 33(3), p 224–230. CrossRef X. Liu, Y. Liu, B. Jin, Y. Lu, and J. Lu, Microstructure Evolution and Mechanical Properties of a SMATed Mg Alloy Under In Situ SEM Tensile Testing, J. Mater. Sci. Technol., 2017, 33(3), p 224–230. CrossRef
10.
Zurück zum Zitat Z. Li, Z. Wen, S. Gu, H. Pei, H. Gao, and Q. Mao, In-Situ Observation of Crack Initiation and Propagation in Ni-Based Superalloy with Film Cooling Holes During Tensile Test, J. Alloys. Compd., 2019, 793, p 65–76. CrossRef Z. Li, Z. Wen, S. Gu, H. Pei, H. Gao, and Q. Mao, In-Situ Observation of Crack Initiation and Propagation in Ni-Based Superalloy with Film Cooling Holes During Tensile Test, J. Alloys. Compd., 2019, 793, p 65–76. CrossRef
11.
Zurück zum Zitat Z. Wang, G. Fang, B. Wang, P. Hu, F. Yi, and S. Meng, Study on Toughening Mechanisms of Pyrolytic Carbon Interface Layer in Cf/ZrB2-SiC Composites Using In-Situ Tensile Experimental and Numerical Methods, J. Eur. Ceram. Soc., 2021, 41(14), p 6791–6804. CrossRef Z. Wang, G. Fang, B. Wang, P. Hu, F. Yi, and S. Meng, Study on Toughening Mechanisms of Pyrolytic Carbon Interface Layer in Cf/ZrB2-SiC Composites Using In-Situ Tensile Experimental and Numerical Methods, J. Eur. Ceram. Soc., 2021, 41(14), p 6791–6804. CrossRef
12.
Zurück zum Zitat S. Hémery, A. Nait-Ali, and P. Villechaise, Combination of In-Situ SEM Tensile Test and FFT-Based Crystal Elasticity Simulations of Ti-6Al-4V for an Improved Description of the Onset of Plastic Slip, Mech. Mater., 2017, 109, p 1–10. CrossRef S. Hémery, A. Nait-Ali, and P. Villechaise, Combination of In-Situ SEM Tensile Test and FFT-Based Crystal Elasticity Simulations of Ti-6Al-4V for an Improved Description of the Onset of Plastic Slip, Mech. Mater., 2017, 109, p 1–10. CrossRef
13.
Zurück zum Zitat M. Taheri, The Fracture Behaviors of the Selective Laser Melting Processed IN738 Superalloy by In-Situ Tensile SEM, Results Opt., 2021, 5, p 100200. CrossRef M. Taheri, The Fracture Behaviors of the Selective Laser Melting Processed IN738 Superalloy by In-Situ Tensile SEM, Results Opt., 2021, 5, p 100200. CrossRef
14.
Zurück zum Zitat M. Taheri, M. Razavi, S.F. Kashani-Bozorg, and M.J. Torkamany, Relationship Between Solidification and Liquation Cracks in the Joining of GTD-111 Nickel-Based Superalloy by Nd: YAG Pulsed-Laser Welding, J. Mater. Res.Technol., 2021, 15, p 5635–5649. CrossRef M. Taheri, M. Razavi, S.F. Kashani-Bozorg, and M.J. Torkamany, Relationship Between Solidification and Liquation Cracks in the Joining of GTD-111 Nickel-Based Superalloy by Nd: YAG Pulsed-Laser Welding, J. Mater. Res.Technol., 2021, 15, p 5635–5649. CrossRef
15.
Zurück zum Zitat M. Taheri, S.F. Kashani-Bozorg, V.V. Ramalingam, B. Babaei, and A. Halvaee, Effect of Nd: YAG Pulsed-Laser Welding Parameters on Melting Rate of GTD-111 Superalloy Joint, J. Mater. Eng. Perform., 2021, 30(12), p 9108–9117. CrossRef M. Taheri, S.F. Kashani-Bozorg, V.V. Ramalingam, B. Babaei, and A. Halvaee, Effect of Nd: YAG Pulsed-Laser Welding Parameters on Melting Rate of GTD-111 Superalloy Joint, J. Mater. Eng. Perform., 2021, 30(12), p 9108–9117. CrossRef
16.
Zurück zum Zitat S.A. Sajjadi, S. Nategh, M. Isac, and S.M. Zebarjad, Tensile Deformation Mechanisms at Different Temperatures in the Ni-Base Superalloy GTD-111, J. Mater. Process. Technol., 2004, 155, p 1900–1904. CrossRef S.A. Sajjadi, S. Nategh, M. Isac, and S.M. Zebarjad, Tensile Deformation Mechanisms at Different Temperatures in the Ni-Base Superalloy GTD-111, J. Mater. Process. Technol., 2004, 155, p 1900–1904. CrossRef
17.
Zurück zum Zitat M. Taheri, A. Halvaee, and S.F. Kashani-Bozorg, Effect of Nd: YAG Pulsed-Laser Welding Parameters on Microstructure and Mechanical Properties of GTD-111 Superalloy Joint, Mater. Res. Express, 2019, 6(7), p 076549. CrossRef M. Taheri, A. Halvaee, and S.F. Kashani-Bozorg, Effect of Nd: YAG Pulsed-Laser Welding Parameters on Microstructure and Mechanical Properties of GTD-111 Superalloy Joint, Mater. Res. Express, 2019, 6(7), p 076549. CrossRef
18.
Zurück zum Zitat H. Huang, G. Liu, H. Wang, Z. Wang, H. Zhang, Y. Shao, and B. Hu, Effect of Cooling Rate and Resulting Microstructure on Tensile Properties and Deformation Mechanisms of an Advanced PM Nickel-Based Superalloy, J. Alloys Compd., 2019, 805, p 1254–1259. CrossRef H. Huang, G. Liu, H. Wang, Z. Wang, H. Zhang, Y. Shao, and B. Hu, Effect of Cooling Rate and Resulting Microstructure on Tensile Properties and Deformation Mechanisms of an Advanced PM Nickel-Based Superalloy, J. Alloys Compd., 2019, 805, p 1254–1259. CrossRef
19.
Zurück zum Zitat Y. Ding, C. Wang, M. Li, and H.S. Bang, Evolution of Deformation Near the Triple Point of Grain Junctions in Sn-Based Solders During in Situ Tensile Test, Mater. Lett., 2005, 59(6), p 697–700. CrossRef Y. Ding, C. Wang, M. Li, and H.S. Bang, Evolution of Deformation Near the Triple Point of Grain Junctions in Sn-Based Solders During in Situ Tensile Test, Mater. Lett., 2005, 59(6), p 697–700. CrossRef
Metadaten
Titel
Fracture Behavior of GTD-111 Superalloy during In Situ Tensile Scanning Electron Microscopy
verfasst von
Yinwei Wang
Pengchao Zhang
Morteza Taheri
Behzad Babaei
Publikationsdatum
18.05.2022
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 12/2022
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-022-07003-z

Weitere Artikel der Ausgabe 12/2022

Journal of Materials Engineering and Performance 12/2022 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.